Department Facilities Details
NMR Spectrometers
JEOL, model Eclipse+ 500
| Description: |
500 MHz 1H, 5 mm probes, variable temperature, inverse detection mode, PFG and pulse shaping |
| Location: |
006 Hahn Hall |
| Contact: |
William Bebout/Tom Glass |
Varian, model Unity 400
| Description: |
400 MHz 1H, multinuclear, 5 & 10 mm probes, variable temperature, inverse detection mode, Sun Ultra 1 data station for data workup |
| Location: |
002 Hahn Hall |
| Contact: |
Tom Glass |
Varian, model Inova 400
| Description: |
400 MHz 1H, multinuclear, 5 mm probes, variable temperature, PFG |
| Location: |
006 Hahn Hall |
| Contact: |
Tom Glass |
Bruker, model MSL-300 Solids Only
| Description: |
75 MHz 13C, multinuclear, 4 & 7 mm MAS probe, variable temperature, Doty 7 mm ultra high temp probe (650 C max.) |
| Location: |
006 Hahn Hall |
| Contact: |
Tom Glass |
NMR Software Tools
NUTS NMR Data Processing Software
| Description: |
1D and 2D offline processing software with internal data translation, relaxation data processing, deconvolution, and spectral simulation |
| Location: |
Hahn 006 running on a Pentium platform, and Davidson 123E departmental computer lab |
| Contact: |
Tom Glass |
ACD/Labs Software Suite
| Description: |
Proton and Carbon spectral calculation, calculation of octanol/water partition coefficients (logP), ChemSketch, ACD Dictionary, and ACD Tautomers |
| Location: |
Hahn 006 running on a Pentium platform |
| Contact: |
Tom Glass |
Mass Spectrometers
Micromass, model Platform LC-MS
| Description: |
Single quad, low resolution, with HP 1050 series LC system |
| Ionization modes: |
Electrospray and APCI |
| Location: |
140 Davidson Hall |
| Contact: |
Dr. Mehdi Ashraf-Khorassani |
Micromass, model Quattro I GC-MS
| Description: |
triple quad, low resolution, with tandem MS, and GC interface to a model 8060 Fison GC |
| Ionization modes: |
70eV EI, methane CI, 20kV Cesium ion FAB, CID, DCI |
| Location: |
006 Hahn Hall |
| Contact: |
Ms. Anne Campbell |
Hewlett Packard, model 5970 MSD GC-MS
| Description: |
Single quad, low resolution, with GC interface to an HP 5890A |
| Ionization modes: |
EI |
| Location: |
006 Hahn Hall |
| Contact: |
Ms. Anne Campbell |
Jeol, model HX110
| Description: |
High resolution double focusing |
| Ionization modes: |
FAB |
| Location: |
127 Davidson Hall |
| Contact: |
William Bebout |
Kratos, Kompact TOF
| Description: |
Matrix-assisted laser desorption/ionization (MALDI) time of flight (TOF) MS |
| Ionization modes: |
MALDI |
| Location: |
106 Engle Hall |
| Contact: |
Kim Harich |
Thermo Finnigan, Quantum AM IC-MS
| Description: |
Triple quad, high resolution with Agilent 1100 series LC |
| Ionization modes: |
ESI, APCI |
| Location: |
127 Davidson Hall |
| Contact: |
Geno Iannaccone |
VG, model 7070E-HF
| Description: |
High resolution double focusing |
| Ionization modes: |
EI/CI, DCI |
| Location: |
106 Engel Hall |
| Contact: |
Kim Harich |
X-Ray Diffractometer
Oxford Diffraction, model Xcalibur2
| Description: |
single crystal, CCD area detector, variable temperature |
| Location: |
3076 Derring Hall |
| Contact: |
Dr. Carla Slebodnick |
UV-Vis Spectroscopy
Perkin-Elmer, model 330
| Description: |
scanning spectrophotometer, 170-2500 nm range, 60 mm integrating sphere accessory |
| Location: |
006 Hahn Hall |
| Contact: |
Geno Iannaccone |
IR Spectroscopy
MIDAC, model M2004
| Description: |
FT-IR spectrophotometer, 6000-400 cm-1 range, high resolution (0.5 cm-1), DTGS detector with ZnSe optics, GRAMS-32 software, diamond HATR accessory. |
| Location: |
006 Hahn Hall |
| Contact: |
Geno Iannaccone |
Perkin-Elmer, model 283B
| Description: |
Dispersive transmission-mode spectrophotometer, 4000-200 cm-1 range, high resolution (0.5 cm-1 at 1000 cm-1), 20-m gas cell accessory |
| Location: |
006 Hahn Hall |
| Contact: |
Geno Iannaccone |
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