CHEM 4114 Instrumental Analysis

Syllabus - Fall 1999

Instructors Course Description Course Outline
         

Instructors

Professor:
Prof. Brian M. Tissue Hahn 1111 / tissue@vt.edu / 231-3786
Office Hours: Wed., Fri. 10:00-10:50 AM
Teaching Assistants:
Brian Trice Hahn 1110 / btrice@vt.edu
Office Hours: posted in lab
Steve Hunsucker Hahn 1009 / shunsuck@vt.edu
Office Hours: posted in lab

Course Description

Text: Skoog, Holler, and Nieman, Principles of Instrumental Analysis 5th Ed.
Prerequisites: CHEM 2114 or 3114, CHEM 3615, CHEM 3616
Credit hours: 4 (The laboratory is mandatory.)

Index #s:
5012  Lecture: Tue. and Thu. / 12:30 - 1:45  / Davidson 412
5013  Lab: Tue. / 2:00 - 4:50 / Davidson 123A
5014  Lab: Thu. / 2:00 - 4:50 / Davidson 123A
5015  Lab: Fri. / 2:00 - 4:50 / Davidson 123A
Note: Keep your schedule free until 6:00pm on your lab day.

This course will cover the principles and applications of analytical instrumentation. The course objectives are to give you (1) an in-depth understanding of the most frequently used analytical methods (the analytical toolbox), (2) an overview to help you choose an appropriate analytical technique for a specific problem, and (3) lots of hands-on experience.

The laboratory assignments will run ahead of the lecture material so that everyone can complete the labs before the exams. To compensate for the dissonance between the lab experiments and the corresponding lecture material, computer prelabs must be completed before coming to laboratory. The prelab assignments and other on-line resources are at: http://www.chem.vt.edu/chem-dept/tissue/4114/. Computers are available in the Davidson Hall computer lab from 8:30am-4:30pm M-F.


Grading
One grade is given for the course, there is not a separate grade for the lab. The +/- system might be used if appropriate.

Pre-lab exercises      5%       First exam           10%
Post-lab summaries     5%       Second exam          10%
Laboratory notebook   40%       Third exam           10%
                                Final exam project   20%
Note: The prelab assignments must be completed by 12 noon on your lab day for credit.

Honor Code
You are expected to abide by the honor code in all work associated with this course. You are encouraged to discuss the course topics and homework problems with each other, however, all work that is turned in for a grade must be done on an individual basis. Falsification of the laboratory notebook (data or TA signoff) is an honor code violation.


Course Outline

Week   Chapter   Topic   Laboratory
1   1, A-1   Introduction, Statistics   statistics
2   6,7   Spectroscopy   spectroscopy
3   8-10   Atomic spectroscopy   spectroscopy
4   13-14   Molecular spectroscopy   spectroscopy
5   15   Fluorescence   spectroscopy
6       Exam 1   chromatography
7   26   Chromatrography   chromatography
8   27   GC   chromatography
9   28,29   HPLC,SFC   chromatography
10   30   Electrophoresis, Exam 2   no lab
11   22   Electrochemistry   electrochemistry
12   23,24   Potentiometry, coulometry   electrochemistry
13   25   Voltammetry   electrochemistry
Thanksgiving Break
14   11,20   Exam 3, Mass spectrometry   mass spectrometry
15   11,20   Mass spectrometry   no lab
    Final   Fri., Dec. 10, 10:05 AM to 12:05 PM