CHEM 4114 Instrumental AnalysisSyllabus - Fall 1999
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| Professor: | |
|---|---|
| Prof. Brian M. Tissue | Hahn 1111 / tissue@vt.edu / 231-3786 Office Hours: Wed., Fri. 10:00-10:50 AM |
| Teaching Assistants: | |
| Brian Trice | Hahn 1110 / btrice@vt.edu Office Hours: posted in lab |
| Steve Hunsucker | Hahn 1009 / shunsuck@vt.edu Office Hours: posted in lab |
Text: Skoog, Holler, and Nieman, Principles of Instrumental Analysis 5th Ed.
Prerequisites: CHEM 2114 or 3114, CHEM 3615, CHEM 3616
Credit hours: 4 (The laboratory is mandatory.)
Index #s: 5012 Lecture: Tue. and Thu. / 12:30 - 1:45 / Davidson 412 5013 Lab: Tue. / 2:00 - 4:50 / Davidson 123A 5014 Lab: Thu. / 2:00 - 4:50 / Davidson 123A 5015 Lab: Fri. / 2:00 - 4:50 / Davidson 123A Note: Keep your schedule free until 6:00pm on your lab day.
This course will cover the principles and applications of analytical instrumentation. The course objectives are to give you (1) an in-depth understanding of the most frequently used analytical methods (the analytical toolbox), (2) an overview to help you choose an appropriate analytical technique for a specific problem, and (3) lots of hands-on experience.
The laboratory assignments will run ahead of the lecture material so that everyone can complete the labs before the exams. To compensate for the dissonance between the lab experiments and the corresponding lecture material, computer prelabs must be completed before coming to laboratory. The prelab assignments and other on-line resources are at: http://www.chem.vt.edu/chem-dept/tissue/4114/. Computers are available in the Davidson Hall computer lab from 8:30am-4:30pm M-F.
Grading
One grade is given for the course, there is not a separate grade for the lab. The +/- system might be used if appropriate.
Pre-lab exercises 5% First exam 10%
Post-lab summaries 5% Second exam 10%
Laboratory notebook 40% Third exam 10%
Final exam project 20%
Note: The prelab assignments must be completed by 12 noon on your lab day for credit.
Honor Code
You are expected to abide by the honor code in all work associated with this course. You are encouraged to discuss the course topics and homework problems with each other, however, all work that is turned in for a grade must be done on an individual basis. Falsification of the laboratory notebook (data or TA signoff) is an honor code violation.
| Week | Chapter | Topic | Laboratory | |||
|---|---|---|---|---|---|---|
| 1 | 1, A-1 | Introduction, Statistics | statistics | |||
| 2 | 6,7 | Spectroscopy | spectroscopy | |||
| 3 | 8-10 | Atomic spectroscopy | spectroscopy | |||
| 4 | 13-14 | Molecular spectroscopy | spectroscopy | |||
| 5 | 15 | Fluorescence | spectroscopy | |||
| 6 | Exam 1 | chromatography | ||||
| 7 | 26 | Chromatrography | chromatography | |||
| 8 | 27 | GC | chromatography | |||
| 9 | 28,29 | HPLC,SFC | chromatography | |||
| 10 | 30 | Electrophoresis, Exam 2 | no lab | |||
| 11 | 22 | Electrochemistry | electrochemistry | |||
| 12 | 23,24 | Potentiometry, coulometry | electrochemistry | |||
| 13 | 25 | Voltammetry | electrochemistry | |||
| Thanksgiving Break | ||||||
| 14 | 11,20 | Exam 3, Mass spectrometry | mass spectrometry | |||
| 15 | 11,20 | Mass spectrometry | no lab | |||
| Final | Fri., Dec. 10, 10:05 AM to 12:05 PM | |||||